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The aim of this study was to evaluate and compare the surface roughness of six esthetic restorative materials (Gradia Direct Anterior, GC Corporation, Tokyo, Japan; Filtek Supreme XTE, 3M ESPE, St. Paul, MN, USA; Ceram.X Universal, Dentsply DeTrey, Konstanz, Germany; Essentia enamel, GC Corporation, Tokyo, Japan; Admira Fusion, Voco, Cuxhaven, Germany; and Estelite, Tokuyama Dental corporation, Taitou-ku, Tokyo, Japan) achieved using three different finishing and polishing techniques.
In this in vitro study Forty specimens of each material (6 mm in diameter, 2 mm high) were created and divided into four groups, one per each finishing and polishing procedure and a control group, only cured and not polished. All specimen preparation and finishing and polishing procedures were performed by the same investigator, to reduce variability, following strictly the manufacturer's instructions. Specimens were analyzed using a profilometer to measure the mean surface roughness (Ra, μm), and microscopy images were taken during the measurements through the microscope of the profilometer. Two-way ANOVA test was applied to determine significant differences with respect to material, finishing/polishing technique, and interaction between both variables. Post hoc comparison was done using Tukey's honestly significant difference test. Significance for statistical tests was predetermined at P < 0.05.
Finishing and polishing procedure using tungsten carbide burs provided the best values in terms of surface roughness. All materials of this study treated with this method have provided superimposable values, and no material can be considered more performing than the others. Similar values were also found in the control group.
This study demonstrated that the finishing technique with carbide burs produced an excellent surface smoothness, even if the best surface smoothness is achieved curing the restorative material under a polyester matrix.
Finishing and polishing procedures are important both from an esthetic point of view and a functional one. Obtaining a well-polished surface of restorative esthetic materials guarantees the esthetics of the restoration and it reduces dental plaque retention.
The size and shape of the filling particles of esthetic restorative materials greatly affect the final surface of the restoration, both in terms of roughness and gloss.
Various techniques of finishing and polishing have been proposed and analyzed over time: many studies have shown that the smoothest surface is obtained using a polyester matrix in direct contact with the material during the curing phase. However, it is not always possible to use this method because of the anatomical complexity of the tooth.
The aim of this in vitro study was to evaluate and compare the surface roughness of esthetic restorative materials achieved using different finishing and polishing techniques.
Specimens' preparation
In this in vitro study one microfilled composite (Gradia Direct Anterior, GC Corporation, Tokyo, Japan), one nanofilled composite (Filtek Supreme XTE, 3M ESPE, St. Paul, MN, USA), one nanoceramic composite (Ceram.X Universal, Dentsply DeTrey, Konstanz, Germany), one ultra-fine hybrid composite (Essentia enamel, GC Corporation, Tokyo, Japan), one nanohybrid Ormocer-based composite (Admira Fusion, Voco, Cuxhaven, Germany), and one supra-nano spherical hybrid composite (Estelite, Tokuyama Dental corporation, Taitou-ku, Tokyo, Japan) were evaluated
All materials were polymerized according to manufacturers' instructions into silicon rings (height 2 mm; internal diameter 6 mm; external diameter 8 mm) to obtain 40 specimens identical in size of each material. Cavities of rings were slightly overfilled with material, covered with transparent polyester film strip (Mylar Strip, Henry Schein, Melville, NY, USA), pressed between glass plates, and polymerized for 40 s on each side using a curing unit (Celalux II, Voco, Cuxhaven, Germany). One light polymerization mode was used for each material standard: 1000 mW/cm 2for 40 s. The intensity of the light was verified with a radiometer (SDS Kerr, Orange, CA, USA). The light was placed perpendicular to the specimen surface, at distance of 1.5 mm. A total of forty specimens of each esthetic restorative material were prepared. After polymerization, the specimens were stored in distilled water at 37°C for 15 days.
Finishing/polishing procedures
The specimens of different esthetic restorative materials were randomly assigned to four groups (10 specimens of each composite for each group): the upper surface of each specimen was finished/polished with different finishing/polishing procedures
Group 1: control group (no finishing/polishing procedures) Group 2: Polishers Kit 4312A – Komet Dental(9403,204,055, 9404,204,055, 9405,204,055) (Komet Brasseler GmbH and Co., Lemgo, Germany). The kit is composed by three different rubber polishers with decreasing abrasiveness Group 3: Polishers Composite Set 4652 – Komet Dental (94025M 204,070, 94025F 204,070) (Komet Brasseler GmbH and Co., Lemgo, Germany). The kit is composed by two different rubber polishers with decreasing abrasiveness Group 4: Polishing Kit 4546 – Komet Dental (H135Q 314,014, 9525UF 204,100) (Komet Brasseler GmbH and Co., Lemgo, Germany). The kit is composed by a carbide tungsten bur and a rubber polisher.
All finishing/polishing procedures were performed by the same investigator, to reduce variability. All these procedures were performed strictly following manufacturer's instructions. At the end of the finishing and polishing procedures, all specimens were thoroughly rinsed with water and allowed to dry for 24 h at 20°C before the average surface roughness (Ra) was measured.
Surface roughness analysis
A profilometer (Alicona Infinite Focus, Alicona Imaging GmbH, Raaba/Graz, Austria) was used to measure the surface roughness of specimens. Ra (surface roughness) was used as unit of measure in this process. Three different types of measurements (Ra) were recorded for each specimen; all the measures were taken from the middle of each specimen, giving a total evaluation length of 1 mm. The mean of all Ra measurement values was calculated for each specimen, and an overall Ra measure was calculated for the total sample group. Microscopy images
Microscopy images (×100) about surface morphology of Gradia Direct Anterior in control group (a), after polishing with REF 4312A (b), REF 4652 (c), and REF 4546 (d). Microscopy images (×100) about surface morphology of Filtek Supreme XTE in control group (a), after polishing with REF 4312A (b), REF 4652 (c), and REF 4546 (d). Microscopy images (×100) about surface morphology of Ceram.X Universal in control group (a), after polishing with REF 4312A (b), REF 4652 (c), and REF 4546 (d). Microscopy images (×100) about surface morphology of Essentia enamel in control group (a), after polishing with REF 4312A (b), REF 4652 (c), and REF 4546 (d). Microscopy images (×100) about surface morphology of Admira Fusion in control group (a), after polishing with REF 4312A (b), REF 4652 (c), and REF 4546 (d). Microscopy images (×100) about surface morphology of Estelite in control group (a), after polishing with REF 4312A (b), REF 4652 (c), and REF 4546 (d).
Statistical analysis
Statistical analysis was performed using computer software (Stata 7.0, StataCorp., Station College, TX, USA). Descriptive statistics including the mean, standard deviation, median, and minimum and maximum Ra values were calculated for each group. Shapiro–Wilk test was used to assess the normality of the distribution with alpha = 0.05. Two-way ANOVA test was applied to determine significant differences with respect to material, finishing/polishing technique, and interaction between both variables. Post hoc comparison was done using Tukey's honestly significant difference test. Significance for statistical tests was predetermined at alpha = 0.05.
Ra values (μm) are presented in
The effectiveness of finishing/polishing procedures on composite surface is an important goal to be achieved in the restorative process. Esthetic restoration can be imperceptible only if its surface closely resembles to the enamel surface.
Two factors affect the quality of polishing: the material used for restoration and the finishing and polishing procedures adopted. As far as the material used is concerned, nano-ceramic composite resin has good mechanical properties with high esthetic features. Their structure is made by small particles clusters, and it gives the possibility to obtain surface smoother than the one obtainable with other materials.
Previous studies have pointed out that the smoothest obtainable surface is obtainable by curing the esthetic material in direct contact with a polyester matrix (Group 1).
On the other hand, as far as the procedures are concerned, among all the finishing and polishing methods investigated in this study, carbide burs (Group 4) are the one that provides the smoother surface and previous studies have confirmed the data obtained.
The least smooth surfaces obtained are those of Groups 2 and 3: the use of rubber polisher alone does not provide a sufficiently smooth surface with respect to the baseline. These results can be explained by the excessive rigidity of the rubber polisher and their gradual wear.
The control group (Group 1) results highlight some differences in surface roughness: these differences are attributable to the different chemical nature of the components of each material and especially to the size of the filler particles.
Considering all the limitations of this in vitro study, it is possible to state that tungsten carbide burs were the most effective ones among the finishing and polishing systems examined. For this reason, tungsten carbide burs are clinically recommended because they are cutting efficient and less time consuming than the other methods. Furthermore, this study highlights the effectiveness of nanofilled restorative materials to achieve the goal of a high level of smoothness. However, it is worth mentioning that further in vitro and in vivo studies on a larger sample of restorative materials are needed to obtain more reliable data.
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Conflicts of interest
The authors of this manuscript declare that they have no conflicts of interest, real or perceived, financial or nonfinancial in this article.